A three-dimensional model for the substrate binding domain of the multidrug ATP binding cassette transporter LmrA

Author(s)
Gerhard Ecker, Karin Pleban, Stephan Kopp, Edina Csaszar, Gerrit J. Poelarends, Monique Putman, Dominik Kaiser, Wilhelmus N. Konings, Peter Chiba
Abstract

Multidrug resistance presents a major obstacle to the treatment of infectious diseases and cancer. LmrA, a bacterial ATP-dependent multidrug transporter, mediates efflux of hydrophobic cationic substrates, including antibiotics. The substrate-binding domain of LmrA was identified by using photo-affinity ligands, proteolytic degradation of LmrA, and identification of ligand-modified peptide fragments with matrix-assisted laser desorption ionization/time of flight mass spectrometry. In the nonenergized state, labeling occurred in the a-helical transmembrane segments (TM) 3, 5 and 6 of the membrane-spanning domain. Upon nucleotide binding, the accessibility of TM5 for substrates increased, whereas that of TM6 decreased. Inverse changes were observed upon ATP-hydrolysis. An atomic-detail model of dimeric LmrA was generated based on the template structure of the homologous transporter MsbA from Vibrio cholerae, allowing a three-dimensional visualization of the substrate-binding domain. Labeling of TM3 of one monomer occurred in a predicted area of contact with TM5 or TM6 of the opposite monomer, indicating substrate-binding at the monomer/monomer interface. Inverse changes in the reactivity of TM segments 5 and 6 suggest that substrate binding and release involves a repositioning of these helices during the catalytic cycle.

Organisation(s)
Department of Biochemistry and Cell Biology
External organisation(s)
Medizinische Universität Wien, University of Groningen
Journal
Molecular Pharmacology
Volume
66
Pages
1169-1179
No. of pages
11
ISSN
0026-895X
DOI
https://doi.org/10.1124/mol.104.001420
Publication date
2004
Peer reviewed
Yes
Austrian Fields of Science 2012
3012 Pharmacy, Pharmacology, Toxicology
Sustainable Development Goals
SDG 3 - Good Health and Well-being
Portal url
https://ucrisportal.univie.ac.at/en/publications/74f0a508-08c4-4b6d-a534-dd9ea180d3bf